Maximizing Sample Recovery with Low-Dead-Volume Autosampler Vials

What is the maximum residual volume of Max Recovery vials

Jul 11, 2023 · Max Recovery vials. The maximum residual volume for a vial depends on what type of injector/autosampler it is used with. Residual volumes are as follows: 10 µL for a 2707 or 2777 Sample Manager. 22 µL for an ACQUITY Fixed Loop (FL) Sample Manager. 22 µL for an Alliance HPLC Sample Manager (Flow Through Needle)

What minimum volume of sample should be in a HPLC vial (2ml

Navid Jubaer The offset is from the default position (approx. 2 mm from the bottom of the vial). A negative offset will result in the needle being lower in the vial when the sample is drawn. A

Shop Total Recovery Vials | Waters

Total Recovery Vials. SKU: 186002630C. LCGC Certified Clear Glass 15 x 45 mm Screw Neck Total Recovery Vial, with Cap and Preslit PTFE/Silicone Septum, 3 mL Volume, 100/pk. Category: VialsContainers&CollectionPlates. Waters Certified vials are tested for cleanliness by HPLC and held to tightest dimensional tolerances in the industry.

hplc vial inserts for autosampler vials 100pics per pack

Oct 13, 2021 · Inserts must be selected based on the inner diameter of the vial neck. Aijiren HPLC vial inserts are ideal for small-volume samples supported by12x32mm vials. The inserts are pre-assembled with polyethylene springs that help align. The tapered design allows for the complete removal of the sample; The flat-bottomed design is affordable.

GUIDELINES FOR AUTOSAMPLER VIAL SELECTION

Sample Volume The amount of sample available for analysis is important in choosing the appropriate vial. If only a limited volume of sample is available, you will have to choose between using an insert for your regular autosampler vial, a microvial or a high recovery vial. Note: Most 12x32 mm autosampler vials hold between 1.5mL to 2.0mL of

Autosampler Vial Inserts | Fisher Scientific

Volume (Metric) 1 – 30of30 Results. 1. Fisherbrand™ 150 μL Spring Insert. Fisherbrand™ spring vial inserts are compatible with 8 mm HPLC and GC autosampler vials. 2. Thermo Scientific™ 9mm Autosampler Inserts. Clear glass or polypropylene inserts for 9mm HPLC and GC autosampler vials are available in a variety of configurations with

0.1ml Polypropylene Low Volume Insert Suit - 2ml Sample Vial

volume vial inserts, when used in conjunction with autosampler vials, allow for maximum sample recovery and easier sample removal.Vial inserts (volume 0.15 mL, glass insert (with bottom spring), O.D. x H 6 mm x 38 mm) allow the use of smaller sample volumes with standard autosampler vials.

Shop Clear Glass Vial | 186002805 | Waters

This vial is able to provide maximum sample capacity (~1 mL) with minimal residual volume (~9 µL). Like all Waters clear glass vials, the material used is Type 1, 33-Expansion borosilicate glass, which is the most chemically inert glass available and generally used in analytical labs that rely on high-quality test results.

Sample Vials and Accessories - Waters Corporation

Vials are tested for high recovery of analytes at 1 ng/mL concentration, using UPLC®/MS/MS (MRM). TruView Vials exhibit the lowest surface adsorption of any LC autosampler vial on the market. 96-Well Plate, 700 µL per well is made from a clean grade of polypropylene. The wells are designed to maximize sample recovery for all ACQUITY UPLC

Autosamplers, Part II — Problems and Solutions

the vial so that you can make maximum use of the sample in the vial. When sample volume is limited, microvials or vial inserts can be used to increase the depth of sample for a given volume. If the needle-depth setting places the needle too far down, the needle can bend when it hits the bottom of the vial. In some instances,

1.5ml Glass High Recovery Vial for Manufacturer - Hplc Vials

2ml 9mm autosampler vials with blue screw caps. China 2ml 12x32mm borosilicate glass hplc vial. 1.5ml Glass High Recovery Vial for Manufacturer. 2ml clear hplc autosampler screw vials. 2ml 12×32 mm borosilicate glass hplc vial price. 0.3ml pp autosampler vials for hplc. 9-425 Autosampler Vials and Accessories.

HPLC Troubleshooting Guide - MilliporeSigma

Recorder gain set too low. Column overloaded. Sample-column interaction. Detector and/or recorder time constants are set too high. Reduce sample volume and/or concentration. Adjust gain. Inject smaller volume (e.g., 10 μL vs. 100 μL) or 1:10 or 1:100 dilution of sample. Change buffer strength, pH, or mobile phase composition.

CMI SEC-MALS Getting Started Guide - Harvard University

o Larger proteins require less sample than smaller proteins. o Typical range 5 – 500 µg/injection § BSA (67 KDa) 100 µl at 2 mg/ml always gives a good light scattering signal • Sample volume: o Maximum injection volume: 100 µl o Minimum injection volume: 5 µl o Glass autosampler vial with low volume insert has 10 µl dead volume.

Autosampler Vials & Caps for HPLC & GC | Thermo Fisher

These are vials are suitable for use when sample volume is limited or when you need to get maximum recovery from the vial. These vials allow small volumes to be sampled accurately by autosamplers with a recoverable volume of much less than 100 µL.